2010.11.1 A unique technique was developed to render dense mullite ceramics with an in situ tough interlocking structure. The microstructures were achieved by using a
Read More2018.12.1 These results suggest that the phase composition and microstructure of mullite ceramics can be tuned by using different milling media, where it is necessary to
Read More2015.9.20 Main members are sillimanite ( x = 0), stoichiometric 3/2-mullite ( x = 0.25), 2/1-mullite ( x = 0.40), and the SiO 2 -free phase ι-alumina ( x = 1, crystal structure not
Read MoreIt is observed that the mullite phase formation, grain growth behavior and microstructure development of the mullite ceramics can be tailored by selecting the milling media
Read More2009.8.1 The objective of this paper was to study the phase formation and microstructure development of mullite from the mixture of Al 2 O 3 and SiO 2, with the
Read More2021.12.2 PDF Mullite is becoming one of the most extensive oxide ceramic materials for advanced structural and functional ceramics because of its remarkable... Find, read and cite all the research you ...
Read More2017.8.25 Introduction. Mullite is one of the ceramic mate1ials, such as alumina, silica, magnesia, calcia, zirco nia, SiC, Si3N4, etc. Among these materials, mullite is one
Read More2023.7.4 Porous mullite ceramics with high porosity (73–86 vol%) have been fabricated with relatively high mechanical strength (up to 22 MPa) and low thermal
Read More2009.8.1 Dense and interlocking microstructures of mullite ceramics were produced from the mixture activated with stainless steel milling media, whereas mullite whiskers
Read More2002.7.17 ... Once the mullite phase is formed before densification to take place, anisotropic grain growth will be allowed, thus producing mullite whiskers. High-energy
Read More2003.7.1 Mullite phase formation and grain growth, in a CuO-doped Al 2 O 3 and silica mixture, has been investigated. The oxide mixture was activated with both stainless steel and tungsten carbide milling media. The milled powders demonstrated a much lower mullite formation temperature when compared to the conventional solid-state reaction
Read More2008.1.1 The outstanding scientific and technical importance of mullite can be explained by. •. Its high thermal stability and the favorable properties like low thermal expansion and conductivity, high creep resistance and corrosion stability together with suitable strength and fracture toughness ( Table 1 ). Table 1.
Read More2018.7.1 The distilled water was used in the milling and washing procedures. As the milling media, zirconia beads with the diameters of 2–5 mm were purchased from Guangzhou Pleased Grinding Media Ltd. Preparation of mullite powders. Fig. 1 shows the flow chart of processing route. To remove the residual carbon, coal fly ash was calcined
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Read More5 天之前 Ceramics Materials. Mullite or porcelainite is a rare silicate mineral formed during contact metamorphism of clay minerals. It can form two stoichiometric forms: 3Al 2 O 3 2SiO 2 or 2Al 2 O 3 SiO 2. Unusually, mullite has no charge-balancing cations present. As a result, there are three different aluminium sites: two distorted tetrahedral and ...
Read More2018.8.15 According to our previous studies, no mullite whisker is formed under the same sintering conditions, if the oxide mixture is just mixed by common milling with ZrO 2 media [26]. Therefore, it is reasonable to believe that all these observations can be attributed to the effect of high-energy mechanochemical activation, due to the use of stainless ...
Read More1998.5.1 Grinding was carried out in isopropyl alcohol in a planetary ball mill (Retsch PM 4, Germany) with a silicon nitride pot and milling media for periods of 70, 135 and 240 h. Weight ratio of milling balls to mullite powder was 1:1. After grinding, the last traces of the solvent were removed at 120°C in a laboratory oven.
Read More2000.12.1 The grinding media was zirconia balls and milling time was 4 hours. After drying, the dried lumps were crushed and passed through the plastic sieve with an aperture size of 149 μm. The particle size and its distribution were determined with a laser particle-size analyzer (LS 230, Coulter Co., USA). ... Mullite is first noticeable in the ...
Read More2009.8.1 This paper reports on phase formation and microstructural development of mullite, derived from B 2 O 3 –Al 2 O 3 –SiO 2 mixtures activated with different milling methods. It is found that the addition of B 2 O 3 has a positive effect on mullite phase formation from the mixture of Al 2 O 3 –SiO 2, which can be qualitatively attributed to the
Read More2001.10.3 Mullite is also a desirable material for high-strength infrared transmitting windows. Protective coatings and electronic substrates are other applications of mullites. Mullite is the
Read More2004.1.1 High-energy ball milling had a great influence on phase formation and morphology development of mullite derived from oxide precursors. Mullite phase was formed at 1300 °C in an oxide mixture of Al 2 O 3 and quartz without high-energy ball milling and the mullitization was not complete up to 1500. °C.. After milling for 5 h, the mullitization
Read More2002.7.17 The oxide mixture was activated with both stainless steel and tungsten carbide milling media. The milled powders demonstrated a much lower mullite formation temperature when compared to the ...
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Read More2008.2.14 Effects of precursor milling on phase evolution and morphology of mullite (3Al 2 O 3 2SiO 2) processed by solid-state reaction have been investigated. Alumina and silica powders were used as starting materials and milling was taken place in a medium energy conventional ball mill and a high-energy planetary ball mill. Milling in a
Read More2009.8.1 This paper reports on phase formation and microstructural development of mullite, derived from B 2 O 3 –Al 2 O 3 –SiO 2 mixtures activated with different milling methods. It is found that the addition of B 2 O 3 has a positive effect on mullite phase formation from the mixture of Al 2 O 3 –SiO 2, which can be qualitatively attributed to the
Read More2003.10.25 The effect of transition metal oxides, including FeO 1.5, CoO and NiO, on the phase formation and morphology development of mullite (3Al 2 O 3 2SiO 2) whiskers from oxide mixtures activated by the high-energy ball milling process, were investigated.With the addition of FeO 1.5, the mullite formation temperature was almost the same as that
Read More2018.9.15 The powder was prepared with 40 wt% dehydroxylated pyrophyllite and 60 wt% alumina to obtain 3:2 mullite. In order to homogeneously mix these powders, the fired pyrophyllite powder was milled for 30 min with 150 ml of isopropanol in an Attritor mill. The alumina balls with 4.5 mm diameter were used as milling media.
Read More1986.1.1 Ball milling media affects the recrystallization of amorphous phases upon subsequent heat treatment. The temperature of recrystallization of zircon and crystallization of zirconia is 30–70°C higher with alumina ball-milling material than with zirconia ball-milling material, from 940 to 950°C and from 880 to 910°C.
Read More1993.5.3 The powders were then milled and comminuted in an attritor mill for 24 hours using mullite as the milling media mixed with 150 ml of distilled water. After the milling was complete the suspension was poured through a 325 mesh sieve and dried in an electric dryer at 100 C. Prior to cold pressing the composites, the powder was broken up, mixed ...
Read More2021.3.23 Mullite (3Al2O32SiO2) is an aluminosilicate characterized by excellent physical properties, which makes it an important ceramic material. In this way, ceramics based on mullite find
Read More2021.9.23 Mullite (3Al 2 O 3 2SiO 2 ) and cordierite (2Al 2 O 3 2MgO5SiO 2 ) are two extremely important phases of this diagram. The former has high thermal and chemical stability, low thermal ...
Read More2018.7.1 The distilled water was used in the milling and washing procedures. As the milling media, zirconia beads with the diameters of 2–5 mm were purchased from Guangzhou Pleased Grinding Media Ltd. 2.2. Preparation of mullite powders. Fig. 1 shows the flow chart of processing route. To remove the residual carbon, coal fly ash was
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Read More1998.11.15 Ball milling media affects the recrystallization of amorphous phases upon subsequent heat treatment. The temperature of recrystallization of zircon and crystallization of zirconia is 30–70°C higher with alumina ball-milling material than with zirconia ball-milling material, from 940 to 950°C and from 880 to 910°C.
Read More1996.1.1 The technology of reaction bonding Al 2 O 3 (RBAO) can be modified by the use of Si-containing additives to yield low-to-zero shrinkage mullite composites. In the present work, SiC particles were added to the Al/Al 2 O 3 precursor mixture. During air heat-treatment, first Al oxidizes to Al 2 O 3 at 300–900 °C, thereafter SiC converts to SiO 2
Read More1998.1.1 The microstructures were achieved by using a commercial mullite powder mechanoactivated with tungsten carbide milling media as seeds and a gel-derived nanosized mullite precursor as a matrix. Only less than 1 wt.% seed was sufficient to trigger the in situ formation of mullite whiskers uniformly distributed in a dense submicron
Read More2020.5.27 Mullite, abu vulkanik, Al2O3, densitas, porositas, kekerasan Abstract: Preparation mullite based on ceramics from volcanic ash and Al 2O 3 by mechanical alloy and sintering method was succesfully. Preparation begins
Read MoreNotes. Mullite is a mineral of long interlocking needle-like crystal structure that is very resistant to thermal shock failure (has a low thermal expansion).It is also has a low thermal conductivity and is very refractory thus the theoretical formula (of 71.8% alumina and 28.2% silica) bears little resemblance to the real world material (we have provided a typical non
Read More2017.8.25 Springer Science+Business Media, LLC 2007 Abstract An Al 2O 3/5 vol.% mullite composite was syn-thesized by using reaction sintering of Al 2O 3/0.78 wt.% SiC at 1,600 C for 2 h in air. The phase analysis of the Al 2O 3/mullite composite was carried out using X-ray dif-fraction (XRD). There were two kinds of mullite in alu-mina/mullite
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